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TitroLine® 7500 KF Trace – Automatic Titrator for Coulometric Water Determination

TitroLine® 7500 KF Trace - Automatic Titrator for Coulometric Water DeterminationThe TitroLine® 7500 KF Trace is a compact, easy-to-use coulometric titrator for water determination according to Karl Fischer (KF) with a typical operating range of 1 ppm – 5% water.

The water determination according to Karl Fisher (KF) is the most selective and precise method for water determination. There is the volumetric and coulometric method. With the volumetric method the iodine is added accurately though a piston burette. The coulometric method generates the iodine directly in the titration vessel which allows the determination of very low water concentrations. The advantage is also that you do not have to determine the concentration of the titrant.

TitroLine® 7500 KF Trace - Automatic Titrator for Coulometric Water Determination

The TitroLine® 7500 KF Trace is a compact, easy-to-use coulometric titrator for water determination according to Karl Fischer (KF) with a typical operating range of 1 ppm – 5% water.

The water determination according to Karl Fisher (KF) is the most selective and precise method for water determination. There is the volumetric and coulometric method. With the volumetric method the iodine is added accurately though a piston burette. The coulometric method generates the iodine directly in the titration vessel which allows the determination of very low water concentrations. The advantage is also that you do not have to determine the concentration of the titrant.

Suitable for chemical, petrochemical and pharmaceutical and other industries. For direct titration in the glass titration vessel the samples must be liquid or gaseous. The water from solid or high viscosity samples needs to be dissolved or extracted externally before or be evaporated by a head space oven TO 7280 or oven + autosampler TO 7280/TW 7650.

The TL 7500 KF trace has an exceptional high visibility full color graphic display which allows viewing even at extreme angles. The titration curve, but also other information such as the temperature of a connected headspace oven are clearly displayed on the display.

The three USB, two RS 232 and Ethernet interfaces makes the TL 7500 KF trace highly communicative. Various USB devices such as printers, barcode readers, keyboards can be connected. Analytical balances, PC and other SI Analytics devices such as the TO 7280 headspace oven can be connected via the RS-232 interfaces. The Ethernet interface allows data to be stored on a directly connected USB stick in PDF and CSV format as well as on shared network directories.

The parameters can be customized in each of the up to 50 methods. Through the user/password management, each user can be assigned individual rights. If you need even more methods or want to manage the data on a PC, you can use the TitriSoft PC software to control the TL 7500 KF trace. The TitriSoft 3.5P (TZ 3572) complies fully with 21 CFR, Part 11.

Benefits of TitroLine® 7500 KF Trace

  • Fast, easy and precise
  • With standard methods for different application (titer, blank value, one or two component reagents)
  • The addition of solvent and the extraction of the titrated sample are managed by the titration stand TM 235 KF (optional for TitroLine® 7500 KF trace)
  • Online display of curve and measurement drift during titration

Key Features TitroLine® 7500 KF Trace

  • Coulometric KF titration with automatic drift determination and correction
  • Standard methods for various applications such as water in%, water in ppm, water with KF oven, etc.
  • Statistical functions including average value and relative standard deviation.
  • Configurable output: Short, Standard with curve, GLP
  • Formula editor for individual calculations
  • Output of results in ppm, %, mg, μg, mg / l. Unit individually adjustable
  • Also suitable for the determination of bromine number
  • The addition of the anolyte and the extraction of the titrated sample are carried out by the accessory Titration Stand (TM 235 KF) at the push of a button (only module 2 and 4)

Specifications TitroLine® 7500 KF Trace

Specifications
Measuring input indicator electrode
Connector for double platium electrode with 2 × 4 mm sockets
Measuring input generator electrode
Sockets: 2 × 4 mm, coded in color
Interfaces:
3 × USB (2 x USB-A and 1 × USB-B), 2 × RS-232-C and 1 x LAN
Display
3.5 inches - 1/4 VGA TFT graphic color display with 320 x 240 pixels
Housing material
Polypropylene
Dimensions
15,3 x 18 x 29,6 cm (W x H x D)
Front keyboard
Polyester coated
Weight
2,3 kg for basic device without magnetic stirrer TM 235 or TM 235 KF
Ambient conditions

Ambient temperature: +10 ... +40 °C for operation and storage Humidity according to EN 61 010, Part 1: max. relative humidity 80% for temperatures up to 31°C, linear decrease down to 50% relative humidity at a temperature of 40°C

Power supply:
100-240 V; 50/60 Hz, power input: 30 VA
CE-sign:

EMC compatibility according to the Council Directive: 2004/108/EG; applied harmonized standards: EN 61326-1:2006
Low-voltage directive according to the Council Directive 2006/95/EG Testing basis EN 61 010, Part 1

Magnetic stirrer TM 235

with Power supply TZ 1855, for vessels up to 500 ml, agitator speed infinitely adjustable from 500 - 2000 r/min, for the connection to TitroLine® 7XXX and TITRONIC® 500

Titration stand TM235 KF

Spesifications
Pump

Free volume flow- air-: flow rate 2.25 l / min
Delivery pressure max. 1.5 bar.
Flow rate liquid medium ca. 0.8 l / min

Stirring speed
50 to 1000 U/min
Hoses

PVC- hose (outer diameter 6 x 1 mm)
PTFE- hose (outer diameter 4 x 0.5 mm)

Dimensions
80 x 130 x 250 mm, (W x H x D (height without stand rod)
Weight
1kg

Titration stand TM235 TO

Spesifications
Pump
Integrated, for supplying the TO 7280 with air from the environment
Stirring speed
50 to 1000 U/min
Valve
Automatically switching valve for air/nitrogen supply
Control
Via USB port by TitroLine® 7500 KF trace titrator
Dimensions
80 x 130 x 250 mm, (W x H x D (height without stand rod)
Weight
1.9 kg

Basic titrator TitroLine® 7500 KF Trace unit includes:

Basic unit, connection cable for generator electrode, connection cable for TM 235, TM 235 KF or TM 235 TO, USB keyboard TZ 3835, retaining clamp TZ 1749 for titration vessel, stand rod TZ 1748 and power supply 100-240 V.

Ordering Information TitroLine® 7500 KF Trace

Type No. Order No. Description
TL 7500KF TRACE M1
285220860

Module 1, coulometric KF titrator, scope of supply: basic titrator unit, generator electrode TZ 1752 without diaphragm + cable, magnetic stirrer TM 235, stand rod, titration vessel TZ 1751, micro double platinum electrode KF 1150

TL 7500KF TRACE M2
285220870

Module 2, coulometric KF titrator, scope of supply: basic titrator unit, generator electrode TZ 1752 without diaphragm + cable, TM 235 KF titration stand with built-in stirrer and pump, stand rod, titration vessel TZ 1754, micro double platin electrode KF

TL 7500KF TRACE M3
285220880

Module 3, coulometric KF titrator, scope of supply: basic titrator unit, generator electrode TZ 1753 with diaphragm + cable, magnetic stirrer TM 235, stand rod, titration vessel TZ 1751, micro double platinum electrode KF 1150

TL 7500KF TRACE M4
285220890

Module 4, coulometric KF titrator, scope of supply: basic titrator unit, generator electrode TZ 1753 with diaphragm + connection cable, TM 235 KF titration stand with built-in stirrer and pump, stand rod, titration vessel TZ 1754, micro double platinum electrode KF 1150

TL 7500KF TRACE M5
285221000

 Module 5, coulometric KF titrator, scope of supply: basic titrator unit, generator electrode TZ 1752 without junction, connection cable, magnetic stirrer TM 235, stand rod, titration vessel TZ 1754, micro double platinum electrode KF 1150.

TL 7500KF TRACE M6
285227800

 Module 6, coulometric KF titrator, scope of supply: basic titrator unit, generator electrode TZ 1752 without junction, connection cable LB 04 NN, TM 235 TO titration stand, stand rod, titration vessel TZ 1754, micro double platinum electrode KF 1150, connection cable TZ 3094

TL 7500KF TRACE M6 TitriSoft Pharma
285227810

 Module 6, coulometric KF titrator, scope of supply: basic titrator unit, generator electrode TZ 1752 without junction, connection cable LB 04 NN, TM 235 TO titration stand, stand rod, titration vessel TZ 1754, micro double platinum electrode KF 1150, connection cable TZ 3094
and TitriSoft 3.5 P

Ordering Information Accessories forTitroLine® 7500 KF Trace

Type No. Order No. Description
WA 05
285220300
5 ml exchangeable unit with integrated chip for reagent data, with brown glass bottle for titrant, GL 45 and S 40-bottle adapter, tubes, drip tube and titration tip
WA 10
285220310
10 ml exchangeable unit with integrated chip for reagent data, with brown glass bottle for titrant, GL 45 and S 40-bottle adapter, tubes, drip tube and titration tip
WA 20
285220320
20 ml exchangeable unit with integrated chip for reagent data, with brown glass bottle for titrant, GL 45 and S 40-bottle adapter, tubes, drip tube and titration tip
WA 50
285220350
50 ml exchangeable unit with integrated chip for reagent data, with brown glass bottle for titrant, GL 45 and S 40-bottle adapter, tubes, drip tube and titration tip
TM 235, 115-230 V
285220400
Content Magnetic stirrer for vessels up to 500 ml, agitator speed infinitely adjustable from 500 - 2000 rpm, for the connection to TitroLine® 6000/7000 and TITRONIC® 500
TM 235 KF, 115-230 V
285220900
Titriation stand with pump; Scope of delivery: Basic unit with 1 l DURAN ®-reagent bottle TZ 1791, 1 l DURAN®-waste bottle TZ 1792, moisture bottle, tubes and screw threads, power supply TZ 1855 (110 to 240 V)
TZ 1052
285214721
KF-drying stove, 230 V
TZ 1055
285215183
KF-drying stove, 115 V
TZ 1060
285218115
Accessories set for KF drying stove TZ 1052/TZ1055
TZ 1065
285201973
Flowmeter with valve and hose connectors for gas volumes (air, nitrogen) from 50 - 500 ml/min
KF 1100
285102030
Micro double platinum electrode for Karl Fischer titrations, with fixed cable, double platinum pin and tapper NS 7.5 for TZ 1770 and TZ 1772
TZ 1748
285216560
Stand rod stainless steel Ø 10 mm
TZ 1770
285216677

Karl Fischer titration vessel. DURAN® glass vessel TZ 1775 (approx. 30...150 ml), removable head made of polypropylene/PTFE, 1 drilling NS 19, NS 14,5, NS 7,5 and 3 drillings with screw threads, titration tip, moisture trap and weighing funnel

TZ 1789
285221120
Starter kit KF consisting of molecular sieve, needles with syringes and glass wool
TZ 3863
285220480
USB-thermo printer, 112 mm for TitroLine® 6000/7000/7500 KF/7500 KF trace/7750 and TITRONIC® 500
TZ 3864
285220710
Thermal paper for TZ 3863 with very high durability (5 rolls)
TZ 3865
285220440
DIN A4 standard printer, HP PCL-compatible, with USB-connection cable, 230 V

More Information

Get more information and English manual for this  Automatic Titrator here!

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